For the experiment sodium boyfriend was used since Its repertories make It easier to be handled. In this experiment both the trans and the CICS Isomers of the 2-methodologically were to be formed. This Is due to the clarity of the compound Itself.
The product will either be thermodynamically controlled or controlled by the kinetics Itself. IR spectroscopy can then be used to determine the conversion of the ketene to alcohols in the experiment. This procedure is very frequently used in the laboratory setting to obtain as accurate of a result as possible.Experimental: Physical data: -Weight of CICS and trans-2-methodologically= 34.
9 g -Weight of empty flask used= 33. 3 g Synthesis of 2-methodologically (mechanism): -Percentage yield of CICS and trans-2-methodologically= *We observed an OH peak at 3350. No carbonyl peak. RFC (methanol with 2-methodologically) = 2. CM/CM= .
CACM RFC (mixture) = 1. CM/3. CM= .
CACM Discussion and conclusion: Our experiment was successful since we managed to get an extra gram of product and hence got rid of the double bond (carbonyl peak) when observing the 1 HON. spectrum.We had a clear formation of alcohol after observing our data; hence our experiment was a success. There was no side reactions observed within our experimental calculations. It was very evident that boyfriend did In fact reduce our Minimal mixture to an alcohol (2-methodologically). In the beginning of the experiment we spilled some of the reacting solution containing boyfriend but we were still able to receive a favorably good result when It came to looking at our final data analysis. References: 1 . Wade Jar.
, L. G. Organic Chemistry.
6th Etalon. New Jersey: Pearson Prentice Hall, 2006.